2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

Base Information

Chemical Name:2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride
CAS No.:120172-80-7
Molecular Formula:C₃₅H₃₁NO₉*ClH
Molecular Weight:646.093
Hs Code.:

Synonyms:2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

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Chemical Property of 2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

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Technology Process of 2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

There total 6 articles about 2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 120172-79-4
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

: 120172-80-7
2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

Guidance literature:: With hydrogenchloride; sodium borohydrid; borane; trifluoroborane diethyl ether; In tetrahydrofuran; methanol; ethyl acetate;

Reference yield: 61.8%

ethereal hydrogen chloride: ethereal hydrogen chloride

: 120172-79-4
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

: 120172-80-7
2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

Guidance literature:: With hydrogenchloride; sodium borohydrid; trifluoroborane diethyl ether; In tetrahydrofuran; methanol; ethyl acetate;

Reference yield:

: 78821-34-8
2,6-dideoxy-2,6-imino-D-glycero-D-ido-heptononitrile

: 120172-80-7
2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / triethylamine / ethyl acetate / 18 h / Ambient temperature

2: 89 percent / triethylamine / ethyl acetate / 1.) 0 deg C, 1 h, 2.) room temperature, 21 h

3: 1.) mercuric trifluoroacetate, 2.) N₂O₄ / 1.) 90percent TFA, room temperature, 3.5 h, 2.) room temperature, 1.5 h

4: 1.) B₂H₆, NaBH₄, BF₃*(C₂H₅)2O, 2.) HCl / 1.) THF, room temperature, 16 h, 2.) anhydrous ether, 0 deg C, 1 h

With hydrogenchloride; sodium tetrahydroborate; boron trifluoride diethyl etherate; mercury(II) trifluoroacetate; dinitrogen tetraoxide; triethylamine; diborane; In ethyl acetate;
DOI:10.1021/jo00272a015