C₁₄H₁₈OS₂

Base Information

Chemical Name:C₁₄H₁₈OS₂
CAS No.:71094-81-0
Molecular Formula:C₁₄H₁₈OS₂
Molecular Weight:266.428
Hs Code.:

C<sub>14</sub>H<sub>18</sub>OS<sub>2</sub>

Synonyms:C₁₄H₁₈OS₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₈OS₂

Chemical Property:

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Technology Process of C₁₄H₁₈OS₂

There total 2 articles about C₁₄H₁₈OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₁₁H₂₃NO₂S₂Si

: 917-54-4
methyllithium

: 100-39-0
benzyl bromide

: 71094-81-0
C₁₄H₁₈OS₂

Guidance literature:: C₁₁H₂₃NO₂S₂Si; methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere;

benzyl bromide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; diethyl ether; at -78 - -30 ℃; Inert atmosphere;
DOI:10.1002/anie.201509342

Reference yield:

: C₉H₁₈O₂S₂Si

: 71094-81-0
C₁₄H₁₈OS₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

2.2: -78 - -30 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; 2.2: |Brook Silaketone Rearrangement;
DOI:10.1002/anie.201509342