4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

Base Information

Chemical Name:4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate
CAS No.:1218810-66-2
Molecular Formula:C₄₆H₆₂O₇
Molecular Weight:726.994
Hs Code.:

Synonyms:4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

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Chemical Property of 4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

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Technology Process of 4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

There total 5 articles about 4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 847223-65-8
4'-(11-hydroxyundecyloxy)-biphenyl-4-carboxylic acid 4-(1-methylheptyloxycarbonyl)-phenyl ester

: 98-89-5
Cyclohexanecarboxylic acid

: 1218810-66-2
4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/c1jm11138h

Reference yield:

: 19812-93-2
4-Cyano-4'-hydroxybiphenyl

: 1218810-66-2
4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / butanone

2: sodium hydroxide / ethanol; water

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; butanone;
DOI:10.1039/c1jm11138h

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 1218810-66-2
4-(1-methylheptyloxycarbonyl)phenyl 4'-[11-(cyclohexylcarbonyloxy)undecyloxy]biphenyl-4-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / butanone

2: sodium hydroxide / ethanol; water

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; butanone;
DOI:10.1039/c1jm11138h