boric acid triphenethyl ester

Base Information

• Chemical Name: boric acid triphenethyl ester
• CAS No.: 29002-70-8
• Molecular Formula: C₂₄H₂₇BO₃
• Molecular Weight: 374.288
• Mol file: 29002-70-8.mol

Synonyms:boric acid triphenethyl ester

Chemical Property of boric acid triphenethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of boric acid triphenethyl ester

There total 7 articles about boric acid triphenethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

ammonia borane + phenylacetaldehyde (122-78-1) → boric acid triphenethyl ester (29002-70-8)

Guidance literature:

In tetrahydrofuran; at 45 ℃; for 3h;

DOI:10.1021/acscatal.0c03294

Reference yield: 13.0%

ammonia borane + phenylacetaldehyde (122-78-1) → 2-phenylethanol (60-12-8) + boric acid triphenethyl ester (29002-70-8)

Guidance literature:

With C₂₈H₂₈Cl₂CoNP₂; In tetrahydrofuran; at 45 ℃; for 3h;

DOI:10.1021/acscatal.0c03294

Reference yield:

styrene oxide (96-09-3) → 2-phenylethanol (60-12-8) + boric acid triphenethyl ester (29002-70-8)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium trifluoromethanesulfonate / tetrahydrofuran / 8 h / 45 °C

2: C₂₈H₂₈Cl₂CoNP₂ / tetrahydrofuran / 3 h / 45 °C

With C₂₈H₂₈Cl₂CoNP₂; lithium trifluoromethanesulfonate; In tetrahydrofuran;

DOI:10.1021/acscatal.0c03294

upstream raw materials:

boric acid tributyl ester

2-phenylethanol

styrene oxide

phenylacetaldehyde