C₃₂H₃₉N₃O₉S

Base Information

Chemical Name:C₃₂H₃₉N₃O₉S
CAS No.:1414948-90-5
Molecular Formula:C₃₂H₃₉N₃O₉S
Molecular Weight:641.742
Hs Code.:

C<sub>32</sub>H<sub>39</sub>N<sub>3</sub>O<sub>9</sub>S

Synonyms:C₃₂H₃₉N₃O₉S

Suppliers and Price of C₃₂H₃₉N₃O₉S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₂H₃₉N₃O₉S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₂H₃₉N₃O₉S

There total 16 articles about C₃₂H₃₉N₃O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1414948-61-0
(1R,3S)-3-(dimethoxymethyl)-1-{(R)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidin-4-yl}-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinolin-8-ol

: 100-39-0
benzyl bromide

: 1414948-90-5
C₃₂H₃₉N₃O₉S

Guidance literature:: With potassium carbonate; In acetone; at 0 - 20 ℃; for 41.5h;
DOI:10.1055/s-0032-1316579

Reference yield:

: 1414948-46-1
(S)-5-(2-amino-3,3-dimethoxypropyl)-2-methoxy-3-methylphenol

: 1414948-90-5
C₃₂H₃₉N₃O₉S

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid; sodium sulfate / dichloromethane / 24 h / 0 - 20 °C

2: potassium carbonate / acetone / 41.5 h / 0 - 20 °C

With formic acid; potassium carbonate; sodium sulfate; In dichloromethane; acetone; 1: |Pictet-Spengler Synthesis;
DOI:10.1055/s-0032-1316579

Reference yield:

: 209624-66-8
3-hydroxy-4-methoxy-5-methylbenzaldehyde

: 1414948-90-5
C₃₂H₃₉N₃O₉S

Guidance literature:: Multi-step reaction with 12 steps

1.1: potassium carbonate / acetone / 2 h / 20 °C

2.1: N,N,N',N'-tetramethylguanidine / dichloromethane / 48 h / 20 °C

3.1: (+)-1,2-bis-[(2S,5S)-2,5-diethylphospholano]benzene (1,5-cycloctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen / ethyl acetate / 72 h / 50 °C / 25858.1 Torr

4.1: methanol; acetyl chloride / 0 - 20 °C

5.1: triethylamine / dichloromethane / 0 - 20 °C

6.1: water; lithium hydroxide / tetrahydrofuran; methanol / 0 - 20 °C

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 0 - 20 °C

8.1: diisobutylaluminium hydride / toluene / 1.5 h / -78 °C / Inert atmosphere

8.2: 1 h / 20 °C

9.1: water; toluene-4-sulfonic acid / methanol / 1.5 h / 20 °C / Reflux

10.1: 10% Pd/C; hydrogen / methanol / 48 h / 20 °C / 760.05 Torr

11.1: formic acid; sodium sulfate / dichloromethane / 24 h / 0 - 20 °C

12.1: potassium carbonate / acetone / 41.5 h / 0 - 20 °C

With methanol; formic acid; (+)-1,2-bis-[(2S,5S)-2,5-diethylphospholano]benzene (1,5-cycloctadiene)rhodium(I) trifluoromethanesulfonate; 10% Pd/C; water; hydrogen; diisobutylaluminium hydride; potassium carbonate; benzotriazol-1-ol; toluene-4-sulfonic acid; sodium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; acetyl chloride; lithium hydroxide; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone; toluene; 2.1: |Horner-Wadsworth-Emmons Olefination / 11.1: |Pictet-Spengler Synthesis;
DOI:10.1055/s-0032-1316579