diisopropyl thiophosphinic chloride

Base Information

• Chemical Name: diisopropyl thiophosphinic chloride
• CAS No.: 23834-61-9
• Molecular Formula: C₆H₁₄ClPS
• Molecular Weight: 184.67
• Mol file: 23834-61-9.mol

Synonyms:diisopropyl thiophosphinic chloride

Chemical Property of diisopropyl thiophosphinic chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diisopropyl thiophosphinic chloride

There total 1 articles about diisopropyl thiophosphinic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetraisopropyldiphosphine monosulfide (62969-12-4) → diisopropyl thiophosphinic chloride (23834-61-9) + Chlorodiisopropylphosphane (40244-90-4)

Guidance literature:

With (Dichloroiodo)benzene;

Reference yield: 54.0%

diisopropyl thiophosphinic chloride (23834-61-9) + P,P-diphenylphosphinothioic amide (17366-80-2) → (C6H5)2P(S)NHP(S)(CH(CH3)2)2 (244181-73-5)

Guidance literature:

P,P-diphenylphosphinothioic amide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 30h;

diisopropyl thiophosphinic chloride; In tetrahydrofuran; at 100 ℃; for 5h; Further stages.;

DOI:10.1039/b103501k

Reference yield: 22.6%

diisopropyl thiophosphinic chloride (23834-61-9) + diphenylphosphoroamidate (2015-56-7) → (C6H5O)2P(O)NHP(S)(CH(CH3)2)2 (386705-09-5)

Guidance literature:

diphenylphosphoroamidate; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

diisopropyl thiophosphinic chloride; In tetrahydrofuran; Further stages.; Heating;

DOI:10.1039/b103501k

upstream raw materials:

tetraisopropyldiphosphine monosulfide

Downstream raw materials:

(C₆H₅O)2P(O)NHP(S)(CH(CH₃)2)2

(C₆H₅)2P(S)NHP(S)(CH(CH₃)2)2

C₁₂H₁₉⁽²⁾HNPS

C₁₃H₂₁⁽²⁾HNPS