N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Base Information

Chemical Name:N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide
CAS No.:1456816-68-4
Molecular Formula:C₁₆H₂₂N₂O₃Se₂
Molecular Weight:448.282
Hs Code.:

Synonyms:N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

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Technology Process of N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

There total 5 articles about N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1456816-58-2
5-(1,2-diselenolan-3-yl)pentanehydrazide

: 121-33-5,8014-42-4
vanillin

: 1456816-68-4
N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Guidance literature:: In ethanol; Reflux;
DOI:10.1080/10426507.2013.765425

Reference yield:

: 6708-13-0
5-(1,2-diselenolan-3-yl)pentanoic acid

: 1456816-68-4
N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / 2 h / 20 °C

1.2: 20 °C

2.1: hydrazine hydrate

3.1: ethanol / Reflux

With hydrazine hydrate; acetyl chloride; In ethanol;
DOI:10.1080/10426507.2013.765425

Reference yield:

: 1451075-56-1
sodium 6,8-dichlorooctanoate

: 1456816-68-4
N'-(3-methoxy-4-hydroxybenzylidene)-5-(1,2-diselenolan-3-yl)pentanehydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: disodium diselenide / ethanol; water / 2 h / 65 °C

1.2: 0 °C / pH 1

2.1: acetyl chloride / 2 h / 20 °C

2.2: 20 °C

3.1: hydrazine hydrate

4.1: ethanol / Reflux

With disodium diselenide; hydrazine hydrate; acetyl chloride; In ethanol; water;
DOI:10.1080/10426507.2013.765425