Technology Process of C20H30O4Si
There total 6 articles about C20H30O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
?chloro[(1S,2S)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine]-(mesitylene) ruthenium (II); formic acid; triethylamine;
In
dichloromethane;
at 20 ℃;
enantioselective reaction;
DOI:10.1016/j.tetlet.2012.06.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic anhydride; dimethyl sulfoxide / 20 °C
2: formic acid; ?chloro[(1S,2S)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine]-(mesitylene) ruthenium (II); triethylamine / dichloromethane / 20 °C
With
?chloro[(1S,2S)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine]-(mesitylene) ruthenium (II); formic acid; acetic anhydride; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
1: Albright-Goldman oxidation;
DOI:10.1016/j.tetlet.2012.06.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 0 °C
1.2: -78 - 0 °C
2.1: acetic anhydride; dimethyl sulfoxide / 20 °C
3.1: formic acid; chloro([(S,2S)-(?)-2-amino-1,2-diphenylethyl](4-toluenesulfonyl)amido)(mesitylene)ruthenium (II); triethylamine / dichloromethane / 20 °C
With
chloro([(S,2S)-(?)-2-amino-1,2-diphenylethyl](4-toluenesulfonyl)amido)(mesitylene)ruthenium (II); n-butyllithium; formic acid; acetic anhydride; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; dichloromethane;
2.1: Albright-Goldman oxidation;
DOI:10.1016/j.tetlet.2012.06.005