(C₅H₅)2Zr(P(CH₃)2C₆H₅)2

Base Information

Chemical Name:(C₅H₅)2Zr(P(CH₃)2C₆H₅)2
CAS No.:71844-72-9
Molecular Formula:C₂₆H₃₂P₂Zr
Molecular Weight:497.712
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)2Zr(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)2

Synonyms:(C₅H₅)2Zr(P(CH₃)2C₆H₅)2

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Chemical Property of (C₅H₅)2Zr(P(CH₃)2C₆H₅)2

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Technology Process of (C₅H₅)2Zr(P(CH₃)2C₆H₅)2

There total 2 articles about (C₅H₅)2Zr(P(CH₃)2C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69058-71-5
(η5-C5H5)2Zr(H)(CH2Cy)

: 672-66-2
Dimethyl(phenyl)phosphine

: 71844-72-9
(C₅H₅)2Zr(P(CH₃)2C₆H₅)2

Guidance literature:: In cyclohexane; byproducts: methylcyclohexane; under Ar phosphine added to Zr-compd./cyclohexane at room temp., stirred for 30 min; product not isolated, detected by NMR;
DOI:10.1021/ja00400a033

Reference yield:

: 69058-71-5
(η5-C5H5)2Zr(H)(CH2Cy)

: 672-66-2
Dimethyl(phenyl)phosphine

: 71844-72-9
(C₅H₅)2Zr(P(CH₃)2C₆H₅)2

: [(η5-cyclopentadienyl)(μ-[eta.1:η5-C5H4])Zr(dimethylphenylphosphine)2]

Guidance literature:: In toluene; byproducts: methylcyclohexane; under Ar phosphine added to Zr-compd./MePh at -80°C, thawed, stirred at room temp. for 1.5 h; frozen, solvent distd., product not sepd., detected by NMR, product ratio dependence to react. time;
DOI:10.1021/ja00400a033