C₂₉H₅₂O₅Si

Base Information

• Chemical Name: C₂₉H₅₂O₅Si
• CAS No.: 1118756-71-0
• Molecular Formula: C₂₉H₅₂O₅Si
• Molecular Weight: 508.814
• Mol file: 1118756-71-0.mol

Synonyms:C₂₉H₅₂O₅Si

Chemical Property of C₂₉H₅₂O₅Si

Chemical Property:

Purity/Quality:

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Technology Process of C₂₉H₅₂O₅Si

There total 1 articles about C₂₉H₅₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C16H33BrO2Si (1118756-69-6) + 1,4-diisopropyloxy-2-methoxybenzene (96501-81-4) → C29H52O5Si (1118756-71-0)

Guidance literature:

1,4-diisopropyloxy-2-methoxybenzene; With n-butyllithium; In tetrahydrofuran; at 20 ℃; for 0.75h;

C₁₆H₃₃BrO₂Si; With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1055/s-0028-1083625

Reference yield: 89.0%

C29H52O5Si (1118756-71-0) → C29H54O5Si (1118756-72-1)

Guidance literature:

With Crabtree's catalyst; hydrogen; In dichloromethane; at 20 ℃; for 12h; under 60006 Torr; optical yield given as %de; diastereoselective reaction;

DOI:10.1055/s-0028-1083625

Reference yield:

C29H52O5Si (1118756-71-0) → C29H54O5Si (1118756-72-1) + C29H54O5Si

Guidance literature:

With palladium on activated charcoal; hydrogen; In ethanol; at 20 ℃; for 12h; under 37503.8 Torr; optical yield given as %de; diastereoselective reaction;

DOI:10.1055/s-0028-1083625

upstream raw materials:

C₁₆H₃₃BrO₂Si

1,4-diisopropyloxy-2-methoxybenzene

Downstream raw materials:

C₂₉H₅₄O₅Si