N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide

Base Information

• Chemical Name: N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide
• CAS No.: 40117-30-4
• Molecular Formula: C₁₁H₁₄ClNO
• Molecular Weight: 211.691
• Mol file: 40117-30-4.mol

Synonyms:N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide

Chemical Property of N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide

There total 10 articles about N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-(4′-chlorobenzyl)-2-methylpropan-2-amine (46234-01-9) → N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide (40117-30-4)

Guidance literature:

With 3,3-dimethyldioxirane; In acetone; at 0 ℃; for 0.166667h;

DOI:10.1021/jo00296a073

Reference yield: 98.0%

N-tertbutylhydroxylamine hydrochloride (57497-39-9) + 4-chlorobenzaldehyde (104-88-1) → N-<(4-Chlorophenyl)methylene>-2-methyl-2-propanamine N-Oxide (40117-30-4)

Guidance literature:

With pyrrolidine; In dichloromethane; at 20 ℃; for 0.333333h; Reagent/catalyst; Solvent;

DOI:10.1021/acscatal.5b01726

Reference yield: 85.0%

N-tert-Butylhydroxylamine (16649-50-6) + 4-chlorobenzaldehyde (104-88-1) → (Z)?N?(tert?butyl)?1?(4?chlorophenyl)methanimine oxide (40117-30-4,137957-45-0)

Guidance literature:

With sodium acetate; at 143 ℃; for 0.0333333h; microwave irradiation;

DOI:10.1016/j.tet.2008.08.101

upstream raw materials:

N-(4′-chlorobenzyl)-2-methylpropan-2-amine

2-tert-butyl-3-(p-chlorophenyl)oxaziridine

(p-chlorobenzylidene)(tert-butyl)amine

N-tertbutylhydroxylamine hydrochloride

Downstream raw materials:

C₁₇H₁₉ClNO

(S)-2-tert-butyl-3-(4-chlorophenyl)-5-phenyl-2,3-dihydroisoxazole-4-carbaldehyde