(4-iodobutyl)anisole

Base Information

Chemical Name:(4-iodobutyl)anisole
CAS No.:75934-24-6
Molecular Formula:C₁₁H₁₅IO
Molecular Weight:290.144
Hs Code.:

Synonyms:(4-iodobutyl)anisole

Suppliers and Price of (4-iodobutyl)anisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
1-(4-Iodobutyl)-2-methoxybenzene 97%
1g
$ 330.00

ACHEMBLOCK
1-(4-Iodobutyl)-2-methoxybenzene 97%
1G
$ 405.00

Total 4 raw suppliers

Chemical Property of (4-iodobutyl)anisole

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1-(4-Iodobutyl)-2-methoxybenzene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-iodobutyl)anisole

There total 1 articles about (4-iodobutyl)anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 628-21-7
1,4-Diiodobutane

: 100-66-3
methoxybenzene

: 75934-24-6
(4-iodobutyl)anisole

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; Yield given. Multistep reaction; 1) in dry ether at reflux for 1h 2) -22 deg C overnight;
DOI:10.1021/jo00317a027

Reference yield: 65.0%

: 75934-24-6
(4-iodobutyl)anisole

: 63667-83-4
1-(but-3-en-1-yl)-2-methoxybenzene

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 90 ℃; for 24h;
DOI:10.1021/jo00317a027

Reference yield:

: 75934-24-6
(4-iodobutyl)anisole

: 4242-18-6
5,6,7,8-tetrahydro-1-naphthalenecarboxylic acid

Guidance literature:: Multi-step reaction with 8 steps

1: potassium tert-butylate / tert-butyl alcohol / 24 h / 90 °C

2: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / 1) in dry ether at reflux for 1h 2) CO₂ as a continous stream for 1h

3: thionyl chloride

4: sodium hydroxide; boron trifluoride-tetrahydrofuran complex; dihydrogen peroxide / 1) for 1h 2) at 50 deg C for 1h

5: triethylamine / dichloromethane / -22 °C

6: lithium bromide / N,N-dimethyl-formamide

7: magnesium / tetrahydrofuran

8: hydrogenchloride / water / 18 h / Heating

With hydrogenchloride; sodium hydroxide; n-butyllithium; thionyl chloride; boron trifluoride-tetrahydrofuran complex; N,N,N,N,-tetramethylethylenediamine; potassium tert-butylate; dihydrogen peroxide; magnesium; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jo00317a027