N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

Base Information

Chemical Name:N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester
CAS No.:2379-12-6
Molecular Formula:C₃₀H₃₁I₂NO₆
Molecular Weight:755.388
Hs Code.:

Synonyms:N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

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Chemical Property of N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

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Technology Process of N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

There total 7 articles about N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2444-23-7
<4-Benzoyloxy-3-tert.-butyl-phenyl>-benzyl-aether

: 2379-12-6
N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C / ethanol

2: MeSO₂Cl

3: (i) (catalytic hydrogenation), (ii) NaNO₂, H₂SO₄, (iii) aq. NaI, I₂, CHCl₃, urea

With hydrogen; methanesulfonyl chloride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00328a012

Reference yield:

: 98-88-4
benzoyl chloride

: 2379-12-6
N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

Guidance literature:: Multi-step reaction with 4 steps

1: (i) aq. NaOH, EtOH, (ii) /BRN= 471389/, Py

2: H₂ / Pd-C / ethanol

3: MeSO₂Cl

4: (i) (catalytic hydrogenation), (ii) NaNO₂, H₂SO₄, (iii) aq. NaI, I₂, CHCl₃, urea

With hydrogen; methanesulfonyl chloride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00328a012

Reference yield:

: 1948-33-0
tert-butylhydroquinone

: 2379-12-6
N-Acetyl-4-O-<4-benzoyloxy-3-tert.-butyl-phenyl>-3,5-diiod-L-tyrosin-aethylester

Guidance literature:: Multi-step reaction with 4 steps

1: (i) aq. NaOH, EtOH, (ii) /BRN= 471389/, Py

2: H₂ / Pd-C / ethanol

3: MeSO₂Cl

4: (i) (catalytic hydrogenation), (ii) NaNO₂, H₂SO₄, (iii) aq. NaI, I₂, CHCl₃, urea

With hydrogen; methanesulfonyl chloride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00328a012