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Technology Process of Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH

Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH

Base Information
  • Chemical Name:Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH
  • CAS No.:88729-94-6
  • Molecular Formula:C35H46CrO6Si
  • Molecular Weight:642.828
  • Hs Code.:
Cr(CO)3C<sub>6</sub>H<sub>3</sub>(OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(CH(CH<sub>2</sub>OH)CH<sub>2</sub>)CHCHCH<sub>2</sub>CH<sub>2</sub>C(CH<sub>3</sub>)CH(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)CH<sub>2</sub>CH<sub>2</sub>CH

Synonyms:Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH

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Chemical Property of Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH
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Technology Process of Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH

There total 1 articles about Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

(3-O-benzyl-17β-O(tert-butyldimethylsilyl)estradiol)-α-tricarbonylchromium
88729-93-5

(3-O-benzyl-17β-O(tert-butyldimethylsilyl)estradiol)-α-tricarbonylchromium

Cr(CO)3C<sub>6</sub>H<sub>3</sub>(OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(CH(CH<sub>2</sub>OH)CH<sub>2</sub>)CHCHCH<sub>2</sub>CH<sub>2</sub>C(CH<sub>3</sub>)CH(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)CH<sub>2</sub>CH<sub>2</sub>CH
88729-94-6

Cr(CO)3C6H3(OCH2C6H5)(CH(CH2OH)CH2)CHCHCH2CH2C(CH3)CH(OSi(CH3)2C(CH3)3)CH2CH2CH

Guidance literature:
With hydrogenchloride; formaldehyd; sodium hexamethyldisilazane; In dimethyl sulfoxide; (Ar); soln. of Cr complex and NaN(SiMe3)2 was stirred at 40°C for 5 min, to mixt. was added formaldehyde at room temp., after 2 h hydrolyzed with aq. HCl; mixt. was extd. with ether and chromd. (silicagel, ether/petroleum ether 1/1); recrystn. from ether/petroleum ether;
DOI:10.1021/ja00319a049
upstream raw materials:

(3-O-benzyl-17β-O(tert-butyldimethylsilyl)estradiol)-α-tricarbonylchromium

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