2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

Base Information

Chemical Name:2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate
CAS No.:1004542-24-8
Molecular Formula:C₆H₈O₇*C₂₅H₂₉N₃
Molecular Weight:563.651
Hs Code.:

Synonyms:2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

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Chemical Property of 2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

Chemical Property:

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Technology Process of 2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

There total 5 articles about 2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004542-23-7
2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile

: 77-92-9,906507-37-7
citric acid

: 1004542-24-8
2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

Guidance literature:: In ethanol; at 20 - 60 ℃;

Reference yield:

: 475098-34-1
4-benzyl-4-(dimethylamino)cyclohexanone

: 1004542-24-8
2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 72 h / 20 °C

1.2: 1 h

2.1: hydrogen / 5%-palladium/activated carbon / methanol / 4.5 h / 40 °C / 2250.23 Torr

3.1: ethanol / 20 - 60 °C

With trifluorormethanesulfonic acid; hydrogen; 5%-palladium/activated carbon; In methanol; ethanol; dichloromethane;

Reference yield:

: 1004547-95-8
3-methyl-5-(trifluoromethyl)-1H-indole

: 1004542-24-8
2-(4-benzyl-4-(dimethylamino)cyclohexyl)-3-methyl-1H-indole-5-carbonitrile citrate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 72 h / 20 °C

1.2: 1 h

2.1: hydrogen / 5%-palladium/activated carbon / methanol / 4.5 h / 40 °C / 2250.23 Torr

3.1: ethanol / 20 - 60 °C

With trifluorormethanesulfonic acid; hydrogen; 5%-palladium/activated carbon; In methanol; ethanol; dichloromethane;