1-(4-ETHOXYPHENYL)ETHANAMINE

Base Information

• Chemical Name: 1-(4-ETHOXYPHENYL)ETHANAMINE
• CAS No.: 104294-63-5
• Molecular Formula: C10H15 N O
• Molecular Weight: 165.23
• Hs Code.: 2922299090
• Mol file: 104294-63-5.mol

Synonyms:Benzylamine,p-ethoxy-a-methyl- (6CI);1-(4-Ethoxyphenyl)-1-ethanamine; 1-(4-Ethoxyphenyl)ethylamine

Chemical Property of 1-(4-ETHOXYPHENYL)ETHANAMINE

Chemical Property:

• Vapor Pressure: 0.014mmHg at 25°C
• Boiling Point: 258.1°Cat760mmHg
• PKA: 9.31±0.10(Predicted)
• Flash Point: 107.4°C
• PSA: 35.25000
• Density: 0.988g/cm³
• LogP: 2.80530

Purity/Quality:

98%min ^*data from raw suppliers

1-(4-Ethoxyphenyl)ethanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-ETHOXYPHENYL)ETHANAMINE

There total 5 articles about 1-(4-ETHOXYPHENYL)ETHANAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(1-azidoethyl)-4-ethoxybenzene → 1-(4-ethoxyphenyl)ethylamine (104294-63-5)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; water; at 70 ℃; for 18h;

Reference yield:

methanesulfonic acid 1-(4-ethoxyphenyl)ethyl ester → 1-(4-ethoxyphenyl)ethylamine (104294-63-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 14 h / 0 - 23 °C

2: triphenylphosphine / tetrahydrofuran; water / 18 h / 70 °C

With sodium azide; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

1-(4-ethoxyphenyl)ethyl alcohol (116071-56-8,52067-36-4,225920-04-7) → 1-(4-ethoxyphenyl)ethylamine (104294-63-5)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 14 h / 0 - 23 °C

2: sodium azide / N,N-dimethyl-formamide / 14 h / 0 - 23 °C

3: triphenylphosphine / tetrahydrofuran; water / 18 h / 70 °C

With sodium azide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

upstream raw materials:

1-(4-ethoxy-phenyl)-ethanone oxime

1-(4-ethoxyphenyl)ethyl alcohol

4-ethoxybenzaldehyde

Refernces