ethyl (E)-3-fluoro-2-phenylacrylate

Base Information

Chemical Name:ethyl (E)-3-fluoro-2-phenylacrylate
CAS No.:85277-78-7
Molecular Formula:C₁₁H₁₁FO₂
Molecular Weight:194.206
Hs Code.:

Synonyms:ethyl (E)-3-fluoro-2-phenylacrylate

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Chemical Property of ethyl (E)-3-fluoro-2-phenylacrylate

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Technology Process of ethyl (E)-3-fluoro-2-phenylacrylate

There total 10 articles about ethyl (E)-3-fluoro-2-phenylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 85278-32-6
ethyl 2-phenyl-3,3-difluoroacrylate

: 85277-78-7
ethyl (E)-3-fluoro-2-phenylacrylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 4-toluenesulfonyl azide; Dimethylphenylsilane; In toluene; at 23 ℃; for 24h; Reagent/catalyst; Temperature; Solvent; stereoselective reaction; Catalytic behavior; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.0c01813

Reference yield: 90.0%

: C₄₇H₄₀FIO₂P₂Pd

: 85277-78-7
ethyl (E)-3-fluoro-2-phenylacrylate

Guidance literature:: With Dimethylphenylsilane; In ⁽²⁾H₈-toluene; at 80 ℃; for 3h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.0c01813

Reference yield:

: 85278-32-6
ethyl 2-phenyl-3,3-difluoroacrylate

: 85277-78-7
ethyl (E)-3-fluoro-2-phenylacrylate

: 2510-99-8
ethyl 2-phenylpropanoate

: 22286-82-4
2-phenyl-acrylic acid ethyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Dimethylphenylsilane; In toluene; at 80 ℃; for 12h; stereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.0c01813