(1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

Base Information

Chemical Name:(1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene
CAS No.:181868-38-2
Molecular Formula:C₃₂H₂₆N₆O₅
Molecular Weight:574.596
Hs Code.:

Synonyms:(1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

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Chemical Property of (1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

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Technology Process of (1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

There total 3 articles about (1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 4157-02-2
cis 2-cyclopentene 1,4-dibenzoate

: 112233-74-6
N₂-acetyl-O₆-(diphenylcarbamoyl)guanine

: Benzoic acid (1S,4R)-4-(2-acetylamino-6-diphenylcarbamoyloxy-purin-7-yl)-cyclopent-2-enyl ester

: Benzoic acid (1R,4S)-4-(2-acetylamino-6-diphenylcarbamoyloxy-purin-9-yl)-cyclopent-2-enyl ester

: 181868-38-2
(1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

Guidance literature:: With 1,2,2,6,6-pentamethylpiperidine; chiral modular ligand; bis(η3-allyl-μ-chloropalladium(II)); In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃;
DOI:10.1021/ja9938837

Reference yield:

: 4157-02-2
cis 2-cyclopentene 1,4-dibenzoate

: 112233-74-6
N₂-acetyl-O₆-(diphenylcarbamoyl)guanine

: Benzoic acid (1S,4R)-4-(2-acetylamino-6-diphenylcarbamoyloxy-purin-7-yl)-cyclopent-2-enyl ester

: 181868-38-2
(1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

: C₄₅H₃₆N₁₂O₆

Guidance literature:: With 1,2,2,6,6-pentamethylpiperidine; chiral modular ligand; bis(η3-allyl-μ-chloropalladium(II)); In tetrahydrofuran; dimethyl sulfoxide; at 0 ℃; for 8h;
DOI:10.1021/ja9938837

Reference yield:

: 4157-02-2
cis 2-cyclopentene 1,4-dibenzoate

: 112233-74-6
N₂-acetyl-O₆-(diphenylcarbamoyl)guanine

: Benzoic acid (1R,4S)-4-(2-acetylamino-6-diphenylcarbamoyloxy-purin-7-yl)-cyclopent-2-enyl ester

: Benzoic acid (1S,4R)-4-(2-acetylamino-6-diphenylcarbamoyloxy-purin-7-yl)-cyclopent-2-enyl ester

: Benzoic acid (1R,4S)-4-(2-acetylamino-6-diphenylcarbamoyloxy-purin-9-yl)-cyclopent-2-enyl ester

: 181868-38-2
(1'R,4'S)-1'-(2-acetamido-6-(N,N-diphenyl)carbamoyloxypurin-9-yl)-4'-benzyloxy-cyclopent-2'-ene

Guidance literature:: With 1,2,2,6,6-pentamethylpiperidine; bis(η3-allyl-μ-chloropalladium(II)); (S,S)-ANDEN-Phenyl Trost Ligand; In dimethyl sulfoxide; at 0 ℃; for 8h; Yield given;