4,6-di-O-acetyl-3-O-D-glucal

Base Information

Chemical Name:4,6-di-O-acetyl-3-O-D-glucal
CAS No.:118356-98-2
Molecular Formula:C₁₀H₁₄O₆
Molecular Weight:230.218
Hs Code.:

Synonyms:4,6-di-O-acetyl-3-O-D-glucal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,6-di-O-acetyl-3-O-D-glucal

Chemical Property:

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Technology Process of 4,6-di-O-acetyl-3-O-D-glucal

There total 3 articles about 4,6-di-O-acetyl-3-O-D-glucal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 2873-29-2
D-glucal triacetate

: 82295-98-5
3,4-di-O-acetyl-1,5-anhydro-2-deoxy-D-arabino-hex-1-enitol

: 118356-98-2
4,6-di-O-acetyl-3-O-D-glucal

Guidance literature:: With lipase of Rhizopus oryze expressed in E_. coli immobilized on octyl-Sepharose; In aq. phosphate buffer; at 25 ℃; for 23h; pH=4.8; regioselective reaction; Enzymatic reaction;
DOI:10.1039/c7cy00255f

Reference yield: 24.0%

: 2873-29-2
D-glucal triacetate

: 63914-23-8
3,6-di-O-acetyl-D-glucal

: 82295-98-5
3,4-di-O-acetyl-1,5-anhydro-2-deoxy-D-arabino-hex-1-enitol

: 118356-98-2
4,6-di-O-acetyl-3-O-D-glucal

Guidance literature:: With lipase of Rhizopus oryze expressed in Pichia pastoris immobilized on octyl-Sepharose N-terminus modified by Boc-Ala-Gly-OH; In aq. phosphate buffer; at 25 ℃; for 24h; pH=4.8; Reagent/catalyst; Solvent; regioselective reaction; Catalytic behavior; Enzymatic reaction;
DOI:10.1039/c7cy00255f

Reference yield:

: 108-24-7
acetic anhydride

: 13265-84-4
D-glucal

: 63914-24-9
6-Monoacetylated D-glucal

: 63914-23-8
3,6-di-O-acetyl-D-glucal

: 118356-98-2
4,6-di-O-acetyl-3-O-D-glucal

: 2873-29-2
D-glucal triacetate

Guidance literature:: With sodium bromide; In N,N-dimethyl-formamide; Yield given. Yields of byproduct given; Ambient temperature; electrolysis: Pt as working el., Ag/Ag(+) in CH₃CN as reference el.;