4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

Base Information

Chemical Name:4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl
CAS No.:111220-64-5
Molecular Formula:C₃₂H₃₀I₂N₂O₆
Molecular Weight:792.409
Hs Code.:

Synonyms:4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

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Chemical Property of 4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

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Technology Process of 4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

There total 6 articles about 4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19177-04-9
1-isopropoxy-3-methylbenzene

: 111220-64-5
4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 52 g / iodine/periodic acid / acetic acid; H₂O; H₂SO₄ / 6 h

2: 16.9 g / copper(I) t-butoxide/pyridine / 1,2-dimethoxy-ethane / 18 h / 75 - 80 °C

3: 3.8 g / Na₂S/NaHCO₃ / H₂O; dioxane / 70 - 100 °C

4: 1.) sulfuric acid/sodium nitrate, 2.) urea, potassium iodide / 1.) sulpholane/water, 0 deg C, 1 h; 2.) sulpholane/water, 0 deg C, 1 h, 90 min

With pyridine; sodium sulfide; sodium nitrate; sulfuric acid; iodine; copper (I) tert-butoxide; sodium hydrogencarbonate; periodic acid; urea; potassium iodide; In 1,4-dioxane; 1,2-dimethoxyethane; sulfuric acid; water; acetic acid;

Reference yield:

: 1820-59-3
2,2',4,4'-tetranitro-1,1'-biphenyl

: 111220-64-5
4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 16.9 g / copper(I) t-butoxide/pyridine / 1,2-dimethoxy-ethane / 18 h / 75 - 80 °C

2: 3.8 g / Na₂S/NaHCO₃ / H₂O; dioxane / 70 - 100 °C

3: 1.) sulfuric acid/sodium nitrate, 2.) urea, potassium iodide / 1.) sulpholane/water, 0 deg C, 1 h; 2.) sulpholane/water, 0 deg C, 1 h, 90 min

With pyridine; sodium sulfide; sodium nitrate; sulfuric acid; copper (I) tert-butoxide; sodium hydrogencarbonate; urea; potassium iodide; In 1,4-dioxane; 1,2-dimethoxyethane; water;

Reference yield:

: 111220-31-6
2-iodo-5-isopropoxytoluene

: 111220-64-5
4'',6'-di-iodo-4,4'''-di-isopropoxy-2',2'''-dimethyl-2',2''-dinitro-m-quaterphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 16.9 g / copper(I) t-butoxide/pyridine / 1,2-dimethoxy-ethane / 18 h / 75 - 80 °C

2: 3.8 g / Na₂S/NaHCO₃ / H₂O; dioxane / 70 - 100 °C

3: 1.) sulfuric acid/sodium nitrate, 2.) urea, potassium iodide / 1.) sulpholane/water, 0 deg C, 1 h; 2.) sulpholane/water, 0 deg C, 1 h, 90 min

With pyridine; sodium sulfide; sodium nitrate; sulfuric acid; copper (I) tert-butoxide; sodium hydrogencarbonate; urea; potassium iodide; In 1,4-dioxane; 1,2-dimethoxyethane; water;