5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester

Base Information

• Chemical Name: 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester
• CAS No.: 183862-79-5
• Molecular Formula: C₃₇H₅₆N₂O₄S₂
• Molecular Weight: 656.995

Synonyms:5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester

Chemical Property of 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester

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Technology Process of 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester

There total 3 articles about 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

methyl adipoyl chloride (35444-44-1) + Hexanoic acid (2-benzylsulfanyl-2-methyl-propyl)-[2-(2-benzylsulfanyl-2-methyl-propylamino)-ethyl]-amide → 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester (183862-79-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/0960-894X(96)00440-4

Reference yield:

Hexanoyl chloride (142-61-0) → 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester (183862-79-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

2: 77 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With triethylamine; In dichloromethane;

DOI:10.1016/0960-894X(96)00440-4

Reference yield:

N,N'-Bis-(2-benzylsulfanyl-2-methyl-propyl)-ethane-1,2-diamine; hydrochloride → 5-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexanoyl-amino]-ethyl}-carbamoyl)-pentanoic acid methyl ester (183862-79-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

2: 77 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With triethylamine; In dichloromethane;

DOI:10.1016/0960-894X(96)00440-4

upstream raw materials:

methyl adipoyl chloride

Hexanoyl chloride

Downstream raw materials:

6-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexyl-amino]-ethyl}-amino)-hexanoic acid methyl ester

6-((2-Benzylsulfanyl-2-methyl-propyl)-{2-[(2-benzylsulfanyl-2-methyl-propyl)-hexyl-amino]-ethyl}-amino)-hexanoic acid

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