(Z)-Cbz-ΔTyr(MOM)-OEt

Base Information

Chemical Name:(Z)-Cbz-ΔTyr(MOM)-OEt
CAS No.:116835-84-8
Molecular Formula:C₂₁H₂₃NO₆
Molecular Weight:385.417
Hs Code.:

Synonyms:(Z)-Cbz-ΔTyr(MOM)-OEt

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Chemical Property of (Z)-Cbz-ΔTyr(MOM)-OEt

Chemical Property:

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Technology Process of (Z)-Cbz-ΔTyr(MOM)-OEt

There total 4 articles about (Z)-Cbz-ΔTyr(MOM)-OEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 116835-81-5
(Z)-ΔTyr(MOM)-OEt

: 116835-84-8
(Z)-Cbz-ΔTyr(MOM)-OEt

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1246/bcsj.61.885

Reference yield:

: 6515-21-5
4-methoxymethoxy-benzaldehyde

: 116835-84-8
(Z)-Cbz-ΔTyr(MOM)-OEt

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / sodium ethoxide / benzene; ethanol / 5-8 deg C, then room temp., 2 h

2: 97 percent / Al-Hg / diethyl ether / reflux, then room temp., 3 h

3: 63 percent / NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 8 h / Ambient temperature

With sodium hydroxide; aluminium amalgam; tetrabutylammomium bromide; sodium ethanolate; In diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1246/bcsj.61.885

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 116835-84-8
(Z)-Cbz-ΔTyr(MOM)-OEt

Guidance literature:: Multi-step reaction with 4 steps

2: 57 percent / sodium ethoxide / benzene; ethanol / 5-8 deg C, then room temp., 2 h

3: 97 percent / Al-Hg / diethyl ether / reflux, then room temp., 3 h

4: 63 percent / NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 8 h / Ambient temperature

With sodium hydroxide; aluminium amalgam; tetrabutylammomium bromide; sodium ethanolate; In diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1246/bcsj.61.885