1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

Base Information

Chemical Name:1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate
CAS No.:1321803-57-9
Molecular Formula:C₂₈H₄₂N₂O₉
Molecular Weight:550.649
Hs Code.:

Synonyms:1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

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Chemical Property of 1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

Chemical Property:

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Technology Process of 1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

There total 3 articles about 1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1321803-56-8
1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

: 1321803-57-9
1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.25h; Inert atmosphere;
DOI:10.1039/c1cc12570b

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1321803-57-9
1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 2.5 h / Reflux

1.2: 1.5 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h

2.2: 2 h / 0 - 20 °C

3.1: dmap; triethylamine / dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere

With dmap; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc12570b

Reference yield:

: 124-04-9
Adipic acid

: 1321803-57-9
1-[N, N, N'-tris((tert-butyloxycarbonyl))hydrazide]-6-benzyl ester adipate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 2.5 h / Reflux

1.2: 1.5 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h

2.2: 2 h / 0 - 20 °C

3.1: dmap; triethylamine / dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere

With dmap; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc12570b