1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

Base Information

Chemical Name:1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate
CAS No.:1321803-56-8
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

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Chemical Property of 1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

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Technology Process of 1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

There total 3 articles about 1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 40542-90-3
adipic acid monobenzyl ester

: 1321803-56-8
1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

Guidance literature:: adipic acid monobenzyl ester; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 0.25h;

t-butoxycarbonylhydrazine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1039/c1cc12570b

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1321803-56-8
1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 2.5 h / Reflux

1.2: 1.5 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h

2.2: 2 h / 0 - 20 °C

With acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1039/c1cc12570b

Reference yield:

: 124-04-9
Adipic acid

: 1321803-56-8
1-[N-(tert-butyloxycarbonyl)hydrazide]-6-benzyl ester adipate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 2.5 h / Reflux

1.2: 1.5 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h

2.2: 2 h / 0 - 20 °C

With acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1039/c1cc12570b