2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide

Base Information

Chemical Name:2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide
CAS No.:1398501-24-0
Molecular Formula:C₁₅H₉Cl₃N₄OS
Molecular Weight:399.688
Hs Code.:

Synonyms:2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide

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Chemical Property of 2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide

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Technology Process of 2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide

There total 2 articles about 2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 883036-00-8
4-(2,3-dichlorophenyl)-3-thiosemicarbazide

: 17630-76-1
5-chloroindole 2,3-dione

: 1398501-24-0
2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide

Guidance literature:: With acetic acid; In ethanol; for 2h; Reflux;
DOI:10.2174/1573406411208030505

Reference yield:

: 6590-97-2
2,3-dichloro-1-isothiocyanatobenzene

: 1398501-24-0
2-(5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene)-N-(2,3-dichlorophenyl)-1-hydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 3 h / Reflux

2: methanol / Reflux

With hydrazine hydrate; In methanol;
DOI:10.1016/j.molstruc.2020.128922