Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

Base Information

Chemical Name:Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone
CAS No.:119517-90-7
Molecular Formula:C₃₀H₂₄N₂O₂
Molecular Weight:444.533
Hs Code.:

Synonyms:Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

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Chemical Property of Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

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Technology Process of Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

There total 4 articles about Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 119517-97-4
1-(4-Biphenylyl)-1-<1-(4-methoxyphenyl)-5-(4-methylphenyl)-3-pyrazolyl>methanol

: 119517-90-7
Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 1h; sonication;
DOI:10.1002/jhet.5570270716

Reference yield:

: 119518-09-1
1-(4-Methoxyphenyl)-5-(4-methylphenyl)pyrazol-3-ylcarboxaldehyde

: 119517-90-7
Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) magnesium, iodine, ethylene bromide / 1.) THF, r.t., 3 h, sonication, 2.) 0 deg C, 1 h

2: 91 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h / sonication

With iodine; magnesium; ethylene dibromide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/jhet.5570270716

Reference yield:

: 119540-34-0
3-Hydroxymethyl-1-(4-methoxyphenyl)-5-(4-methylphenyl)pyrazole

: 119517-90-7
Biphenyl-4-yl-[1-(4-methoxy-phenyl)-5-p-tolyl-1H-pyrazol-3-yl]-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / chromium trioxide, pyridine / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) r.t., 7 h

2: 1.) magnesium, iodine, ethylene bromide / 1.) THF, r.t., 3 h, sonication, 2.) 0 deg C, 1 h

3: 91 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h / sonication

With pyridine; chromium(VI) oxide; iodine; magnesium; ethylene dibromide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/jhet.5570270716