C₃₁H₄₂N₄O₉S

Base Information

Chemical Name:C₃₁H₄₂N₄O₉S
CAS No.:1414916-03-2
Molecular Formula:C₃₁H₄₂N₄O₉S
Molecular Weight:646.762
Hs Code.:

C<sub>31</sub>H<sub>42</sub>N<sub>4</sub>O<sub>9</sub>S

Synonyms:C₃₁H₄₂N₄O₉S

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Chemical Property of C₃₁H₄₂N₄O₉S

Chemical Property:

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Technology Process of C₃₁H₄₂N₄O₉S

There total 5 articles about C₃₁H₄₂N₄O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39895-56-2
4-hydroxymethyl-benzylamine

: 1414916-03-2
C₃₁H₄₂N₄O₉S

Guidance literature:: Multi-step reaction with 8 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 6.5 h / 0 - 20 °C / Inert atmosphere

2: manganese(IV) oxide / tetrahydrofuran / Inert atmosphere

3: sodium cyanoborohydride / methanol / 4 h / 20 °C / Inert atmosphere

4: dichloromethane / 20 °C

5: triethylsilane; trifluoroacetic acid / dichloromethane / 3 h / 20 °C

6: isopropyl alcohol; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C

7: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 4 h / 20 °C

8: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C

With triethylsilane; manganese(IV) oxide; palladium 10% on activated carbon; sodium cyanoborohydride; hydrogen; N-ethyl-N,N-diisopropylamine; isopropyl alcohol; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm301058f

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1449432-51-2
C₂₆H₃₄N₄O₇S

: 1414916-03-2
C₃₁H₄₂N₄O₉S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 6h;
DOI:10.1021/jm301058f

Reference yield:

: 1414915-97-1
(R)-dimethyl-2-(4-((4-methoxy-2,3,6-trimethylphenylsulfonamido)methyl)benzylamino)succinate

: 1414916-03-2
C₃₁H₄₂N₄O₉S

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 20 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane / 3 h / 20 °C

3: isopropyl alcohol; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 4 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C

With triethylsilane; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; isopropyl alcohol; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm301058f