dibutylphenylstannyl bromide

Base Information

Chemical Name:dibutylphenylstannyl bromide
CAS No.:2322-57-8
Molecular Formula:C₁₄H₂₃BrSn
Molecular Weight:389.951
Hs Code.:

Synonyms:dibutylphenylstannyl bromide

Suppliers and Price of dibutylphenylstannyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of dibutylphenylstannyl bromide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of dibutylphenylstannyl bromide

There total 13 articles about dibutylphenylstannyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2170-05-0
pentaphenylantimony

: 996-08-7
dibutyltin dibromide

: 2322-57-8
dibutylphenylstannyl bromide

: 16894-69-2
tetraphenylantimony(V) bromide

Guidance literature:: In toluene; mixt. of equimolar amts. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of Ph4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal.;

Reference yield: 74.0%

: 6452-61-5
di-n-butyldiphenyltin

: 2322-57-8
dibutylphenylstannyl bromide

Guidance literature:: With Br₂; In chloroform; byproducts: bromobenzene; dropwise addn. of soln. of Br2 in CHCl3 to soln. of Sn-compd. in the same solvent with stirring; removal of solvent under vac., distn. under vac. of residue gives bromobenzene and the tin-compd., elem. anal.;
DOI:10.1039/DT9940002135