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Technology Process of (rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)

(rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)

Base Information
  • Chemical Name:(rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)
  • CAS No.:1036029-58-9
  • Molecular Formula:C32H12BF24*C48H38NPRh
  • Molecular Weight:1625.94
  • Hs Code.:
(rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh<sub>3</sub>)(B(3,5-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4)

Synonyms:(rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)

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Chemical Property of (rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)
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Technology Process of (rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)

There total 1 articles about (rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Rh(PPh<sub>3</sub>)(trop<sub>2</sub>NH)][trifluoromethanesulfonate]
872203-30-0

[Rh(PPh3)(trop2NH)][trifluoromethanesulfonate]

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
79060-88-1

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

(rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh<sub>3</sub>)(B(3,5-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4)
1036029-58-9

(rhodium(I))(bis(5-H-dibenzo[a,d]cyclopenten-5-yl)amine)(PPh3)(B(3,5-(CF3)2C6H3)4)

Guidance literature:
In dichloromethane; byproducts: NaOTf; under Ar; Rh complex and B compd. dissolved in CH2Cl2; soln. stirred for2 h; NaOTf removed by filtration; solvent removed under reduced pressur e; washed with pentane; dried in vac.;
DOI:10.1002/anie.200704685
upstream raw materials:

[Rh(PPh3)(trop2NH)][trifluoromethanesulfonate]

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

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