1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

Base Information

Chemical Name:1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine
CAS No.:1174758-26-9
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

Synonyms:1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

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Chemical Property of 1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

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Technology Process of 1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

There total 1 articles about 1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 930-22-3,62249-81-4
epoxybutene

: 1174758-20-3
1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

: 1174758-26-9
1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

Guidance literature:: 1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N,N’-(1S,2S)-cyclohexane-1,2-diylbis[2-(diphenylphosphino)-1-naphthamide]; tetrabutylammomium bromide; In acetonitrile; for 0.166667h; Inert atmosphere;

epoxybutene; In acetonitrile; at 0 ℃; for 20h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol901185d

Reference yield: 91.0%

: 1174758-26-9
1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

: 1174758-38-3
(R)-3-hydroxymethyl-3,6-dihydropyridazine-1,2-dicarboxylic acid dibenzyl ester

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 - 40 ℃; for 61h; Inert atmosphere;
DOI:10.1021/ol901185d