1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

Base Information

Chemical Name:1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine
CAS No.:1174758-20-3
Molecular Formula:C₁₉H₂₀N₂O₄
Molecular Weight:340.379
Hs Code.:

Synonyms:1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

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Technology Process of 1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

There total 1 articles about 1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 5394-50-3
bis(phenylmethyl) 1,2-hydrazinedicarboxylate

: 106-95-6
allyl bromide

: 1174758-20-3
1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

: 186419-15-8
C₂₂H₂₄N₂O₄

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol901185d

Reference yield: 79.0%

: 930-22-3,62249-81-4
epoxybutene

: 1174758-20-3
1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine

: 1174758-26-9
1-allyl-1-benzyloxycarbonyl-2-((R)-1-hydroxymethylallyl)-2-benzyloxycarbonyl hydrazine

Guidance literature:: 1-allyl-1-benzyloxycarbonyl-2-benzyloxycarbonyl hydrazine; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N,N’-(1S,2S)-cyclohexane-1,2-diylbis[2-(diphenylphosphino)-1-naphthamide]; tetrabutylammomium bromide; In acetonitrile; for 0.166667h; Inert atmosphere;

epoxybutene; In acetonitrile; at 0 ℃; for 20h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol901185d