3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-N^α-Z-L-Tyr)-amido-Z-stilbene

Base Information

• Chemical Name: 3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-N^α-Z-L-Tyr)-amido-Z-stilbene
• CAS No.: 865717-76-6
• Molecular Formula: C₃₈H₄₀N₂O₈
• Molecular Weight: 652.744

Synonyms:3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-N^α-Z-L-Tyr)-amido-Z-stilbene

Chemical Property of 3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-N^α-Z-L-Tyr)-amido-Z-stilbene

Chemical Property:

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Technology Process of 3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-N^α-Z-L-Tyr)-amido-Z-stilbene

There total 1 articles about 3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-N^α-Z-L-Tyr)-amido-Z-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine (5545-54-0) + 2-Methoxy-5-[(Z)-2-(7-methoxy-benzo[1,3]dioxol-5-yl)-vinyl]-phenylamine (501033-98-3) → 3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-Nα-Z-L-Tyr)-amido-Z-stilbene (865717-76-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 0.75h;

DOI:10.1021/np058033l

Reference yield:

3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-Nα-Z-L-Tyr)-amido-Z-stilbene (865717-76-6) → C34H32N2O8

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.333333h;

DOI:10.1021/np058033l

Reference yield:

3,4-methylenedioxy-5,4'-dimethoxy-3'-(O-tert-butyl-Nα-Z-L-Tyr)-amido-Z-stilbene (865717-76-6) → C34H31ClN2O7

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 0.33 h

2: tetrachloromethane / acetonitrile / 0.17 h / -10 °C

With tetrachloromethane; trifluoroacetic acid; In dichloromethane; acetonitrile;

upstream raw materials:

N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

2-Methoxy-5-[(Z)-2-(7-methoxy-benzo[1,3]dioxol-5-yl)-vinyl]-phenylamine

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