5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride

Base Information

Chemical Name:5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride
CAS No.:76659-82-0
Molecular Formula:C₁₃H₁₅N₅O*ClH
Molecular Weight:294.748
Hs Code.:

Synonyms:5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride

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Technology Process of 5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride

There total 2 articles about 5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76659-81-9
5-(Formyl-d-benzylamino)-N'-methoxy-1-methyl-1H-imidazole-4-carboxamidine

: 76659-82-0
5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; nickel; at 21 ℃; for 8h; under 760 Torr;
DOI:10.1248/cpb.38.99

Reference yield:

: 70276-45-8
5-(Formylbenzylamino)-N'-methoxy-1-methyl-1H-imidazole-4-carboxamidine

: 76659-82-0
5-(Formyl-d-benzylamino)-1-methyl-1H-imidazole-4-carboxamidine Hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / 1N aq. NaOH / 1 h / Heating

2: 80 percent / acetonitrile / 118 h / 30 °C

3: H₂, HCl / Ni(Raney) / H₂O / 8 h / 21 °C / 760 Torr

With hydrogenchloride; sodium hydroxide; hydrogen; Ni(Raney); In water; acetonitrile;