11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

Base Information

Chemical Name:11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate
CAS No.:1425539-79-2
Molecular Formula:C₃₃H₄₃NO₆
Molecular Weight:549.708
Hs Code.:

Synonyms:11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

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Chemical Property of 11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

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Technology Process of 11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

There total 6 articles about 11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 760-93-0
methacryloyl anhydride

: (2Z)-2-(3,5-diethoxy)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile

: 1425539-79-2
11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

Guidance literature:: (2Z)-2-(3,5-diethoxy)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile; With dmap; triethylamine; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

methacryloyl anhydride; at 5 - 20 ℃; for 19h;

Reference yield: 39.0%

: 760-93-0
methacryloyl anhydride

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 1425539-79-2
11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; methanol; water;

Reference yield:

: 1126-62-1
(3,4-dihydroxy-phenyl)-acetonitrile

: 1425539-79-2
11-{4-[(Z)-2-cyano-2-(3,4-dimethoxyphenyl)ethenyl]-2-methoxyphenoxy}undecyl 2-methylacrylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 6 h / 80 °C

2.1: potassium tert-butylate; hydrogenchloride / tert-butyl methyl ether / 17.5 h / 54 °C

3.1: dmap; triethylamine / tetrahydrofuran / 0 °C / Inert atmosphere

3.2: 19 h / 5 - 20 °C

With hydrogenchloride; dmap; potassium tert-butylate; potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; tert-butyl methyl ether; N,N-dimethyl-formamide;