1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

Base Information

Chemical Name:1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene
CAS No.:312608-06-3
Molecular Formula:C₁₇H₂₆O₇
Molecular Weight:342.389
Hs Code.:

Synonyms:1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

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Chemical Property of 1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

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Technology Process of 1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

There total 5 articles about 1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 106-95-6
allyl bromide

: 312608-04-1
2,4-dimethoxyethoxymethyloxyphenol

: 312608-06-3
1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

Guidance literature:: With potassium carbonate; In acetone; for 6h; Heating;
DOI:10.1016/S0957-4166(00)00302-5

Reference yield:

: (2,4-dihydroxy-benzylidene)-dimethyl-ammonium; dichloro phosphate

: 312608-06-3
1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: H₂O / 0.5 h / 50 °C

2: 90 percent / N,N'-diisopropylethylamine / tetrahydrofuran / 2 h / 20 °C

3: 80 percent / m-CPBA / ethyl acetate / 24 h / 20 °C

4: 85 percent / K₂CO₃ / acetone / 6 h / Heating

With water; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethyl acetate; acetone; 1: Hydrolysis / 2: Alkylation / 3: Oxidation / 4: allylation;
DOI:10.1016/S0957-4166(00)00302-5

Reference yield:

: 141330-16-7
2,4-Bis<(2-methoxyethoxy)methoxy>benzaldehyd

: 312608-06-3
1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / m-CPBA / ethyl acetate / 24 h / 20 °C

2: 85 percent / K₂CO₃ / acetone / 6 h / Heating

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethyl acetate; acetone; 1: Oxidation / 2: allylation;
DOI:10.1016/S0957-4166(00)00302-5