2,4-dimethoxyethoxymethyloxyphenol

Base Information

• Chemical Name: 2,4-dimethoxyethoxymethyloxyphenol
• CAS No.: 312608-04-1
• Molecular Formula: C₁₄H₂₂O₇
• Molecular Weight: 302.324
• Mol file: 312608-04-1.mol

Synonyms:2,4-dimethoxyethoxymethyloxyphenol

Chemical Property of 2,4-dimethoxyethoxymethyloxyphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dimethoxyethoxymethyloxyphenol

There total 4 articles about 2,4-dimethoxyethoxymethyloxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2,4-Bis<(2-methoxyethoxy)methoxy>benzaldehyd (141330-16-7) → 2,4-dimethoxyethoxymethyloxyphenol (312608-04-1)

Guidance literature:

2,4-Bis<(2-methoxyethoxy)methoxy>benzaldehyd; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;

With water; potassium hydroxide; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c2cc36861g

Reference yield:

2,4-Dihydroxybenzaldehyde (95-01-2) → 2,4-dimethoxyethoxymethyloxyphenol (312608-04-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / N,N'-diisopropylethylamine / tetrahydrofuran / 2 h / 20 °C

2: 80 percent / m-CPBA / ethyl acetate / 24 h / 20 °C

With N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethyl acetate; 1: Alkylation / 2: Oxidation;

DOI:10.1016/S0957-4166(00)00302-5

Reference yield:

(2,4-dihydroxy-benzylidene)-dimethyl-ammonium; dichloro phosphate → 2,4-dimethoxyethoxymethyloxyphenol (312608-04-1)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂O / 0.5 h / 50 °C

2: 90 percent / N,N'-diisopropylethylamine / tetrahydrofuran / 2 h / 20 °C

3: 80 percent / m-CPBA / ethyl acetate / 24 h / 20 °C

With water; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethyl acetate; 1: Hydrolysis / 2: Alkylation / 3: Oxidation;

DOI:10.1016/S0957-4166(00)00302-5

upstream raw materials:

2,4-Bis<(2-methoxyethoxy)methoxy>benzaldehyd

2,4-Dihydroxybenzaldehyde

recorcinol

Downstream raw materials:

1-allyloxy-2,4-dimethoxyethoxymethyloxybenzene

4,4'-(((4-bromo-1,3-phenylene)bis(methylene))bis(oxy))bis(1,3-bis((2-methoxyethoxy)methoxy)benzene)

1,2,4-Trihydroxybenzene

4-(2-nitrobenzyloxy)-1,3-phenylene diacetate