meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

Base Information

Chemical Name:meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)
CAS No.:1374660-06-6
Molecular Formula:C₄₈H₇₁O₉P
Molecular Weight:823.06
Hs Code.:

Synonyms:meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

Chemical Property:

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Technology Process of meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

There total 6 articles about meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: didecyl N,N-diisopropylphosphoramidite

: 129952-31-4,130009-54-0
(+/-)-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol

: 1374660-06-6
meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

Guidance literature:: didecyl N,N-diisopropylphosphoramidite; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

(+/-)-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol; In dichloromethane; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; Cooling with ice; Inert atmosphere;

Reference yield:

: C₄₈H₇₁O₈P

: 1374660-06-6
meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c2ob00031h

Reference yield:

: 100-39-0
benzyl bromide

: 1374660-06-6
meso-2,4,6-tri-O-benzyl-1,3-O-methylidene-D-myo-inositol-5-(didecyl phosphate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3.1: 1H-tetrazole / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-tetrazole; sodium hydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2ob00031h