Technology Process of (E) 3-Methyl-5-(2,2,6-trimethylcyclohexen-1-yl)-2-pentenoic Acid
There total 11 articles about (E) 3-Methyl-5-(2,2,6-trimethylcyclohexen-1-yl)-2-pentenoic Acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol; water;
for 18h;
Heating;
DOI:10.1055/s-1982-29808
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / H2 / Raney nickel W5 / ethanol / 24 h / 120 °C / 38000 Torr
2: 96 percent / H2SO4 aq / methanol / 2 h / Ambient temperature
3: 90 percent / Na2Cr2O7*H2O, H2SO4 conc. / benzene; H2O; acetic acid / Ambient temperature
4: 1.) NaH / 1.) THF, room temp., 1 h, 2.) THF, room temp., 18 h
5: 89 percent / 1.) KOH / ethanol; H2O / 18 h / Heating
With
potassium hydroxide; sodium dichromate; sulfuric acid; hydrogen; sodium hydride;
Raney nickel W5;
In
methanol; ethanol; water; acetic acid; benzene;
DOI:10.1055/s-1982-29808
- Guidance literature:
-
methyl (E,E)-farnesoate;
With
fluorosulphonic acid; 1-butyl-3-methylimidazolium Tetrafluoroborate;
In
dichloromethane;
at -45 ℃;
for 0.5h;
With
potassium hydroxide;
for 2h;
Further stages.;
Heating;
DOI:10.1007/s10600-006-0175-6
