1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

Base Information

Chemical Name:1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole
CAS No.:82980-21-0
Molecular Formula:C₂₁H₂₂N₂O₃S
Molecular Weight:382.483
Hs Code.:

Synonyms:1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

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Chemical Property of 1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

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Technology Process of 1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

There total 3 articles about 1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 82980-20-9
1-Benzenesulfonyl-3-[2-(3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

: 82980-21-0
1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; for 1h; Ambient temperature;
DOI:10.1021/jo00144a009

Reference yield:

: 24716-24-3
N-<β-(3-indolyl)ethyl>-3-ethylpyridinium bromide

: 82980-21-0
1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / tetra-n-butylammonium hydrogen sulfate, 50percent aq. NaOH / benzene; H₂O / 1 h / Ambient temperature

2: 91 percent / m-chloroperbenzoic acid, sodium bicarbonate / CH₂Cl₂; H₂O / 1 h / Ambient temperature

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; benzene;
DOI:10.1021/jo00144a009

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 82980-21-0
1-Benzenesulfonyl-3-[2-(1-oxy-3,6-dihydro-2H-pyridin-1-yl)-ethyl]-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / tetra-n-butylammonium hydrogen sulfate, 50percent aq. NaOH / benzene; H₂O / 1 h / Ambient temperature

2: 91 percent / m-chloroperbenzoic acid, sodium bicarbonate / CH₂Cl₂; H₂O / 1 h / Ambient temperature

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; benzene;
DOI:10.1021/jo00144a009