1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

Base Information

Chemical Name:1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate
CAS No.:953053-78-6
Molecular Formula:C₂₉H₃₂N₂O₅S
Molecular Weight:520.649
Hs Code.:

Synonyms:1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

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Chemical Property of 1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

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Technology Process of 1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

There total 4 articles about 1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 953053-76-4
4-methyl-N-[[2-[(1E)-(phenylmethoxy)imino]methyl]phenyl]benzenesulfonamide

: 86606-04-4
(E)-tert-butyl 4-bromobut-2-enoate

: 953053-78-6
1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃;
DOI:10.1016/j.tet.2007.07.007

Reference yield:

: (2E)-4-[[(4-methylphenyl)sulfonyl][2-[(phenylmethoxy)imino]methyl]phenyl]amino-N-(phenylmethyl)-2-butanamide

: 953053-78-6
1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 8 percent / Bu₃SnH; AIBN / benzene / 5 h / Heating

2: 89 percent / K₂CO₃ / acetone / 20 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; In acetone; benzene;
DOI:10.1016/j.tet.2007.07.007

Reference yield:

: 6590-65-4
N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide

: 953053-78-6
1,1-dimethyl-(2E)-4-[[(4-methylphenyl)sulfonyl][2-(1E)-[(phenylmethoxy)imino]methyl]phenyl]amino-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.92 g / sodium acetate / CH₂Cl₂; methanol / 1.5 h / 20 °C

2: 89 percent / K₂CO₃ / acetone / 20 °C

With sodium acetate; potassium carbonate; In methanol; dichloromethane; acetone;
DOI:10.1016/j.tet.2007.07.007