(2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

Base Information

Chemical Name:(2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone
CAS No.:767319-48-2
Molecular Formula:C₁₉H₂₈O₃
Molecular Weight:304.43
Hs Code.:

Synonyms:(2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

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Chemical Property of (2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

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Technology Process of (2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

There total 1 articles about (2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 767319-40-4
(-)-(1Z,2S,3R,4R)-1-ethylidene-2,4-dimethyl-5-oxo-3-((1S)-1-phenylethoxy)-heptyl isobutyrate

: 767319-48-2
(2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

Guidance literature:: With tributyltin methoxide; at 70 ℃; for 12h; under 0.1 Torr;
DOI:10.1021/ol048988f

Reference yield: 80.0%

: 767319-48-2
(2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

: 767319-50-6
(-)-(1R,2R,3R,4R,5R,6R)-1-ethyl-2,4,6-trimethyl-5-((1S)-1-phenylethoxy)cyclohexan-1,3-diol

Guidance literature:: With L-Selectride; In tetrahydrofuran; at -78 ℃; for 24h;
DOI:10.1021/ol048988f

Reference yield:

: 767319-48-2
(2S,3S,4R,5S,6S)-3-Ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexanone

: (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (1R,2R,3S,4R,5R,6S)-3-ethyl-3-hydroxy-2,4,6-trimethyl-5-((S)-1-phenyl-ethoxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / L-selectride / tetrahydrofuran / 24 h / -78 °C

2: pyridine / -20 - 20 °C

With pyridine; L-Selectride; In tetrahydrofuran;
DOI:10.1021/ol048988f