7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

Base Information

Chemical Name:7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate
CAS No.:1351592-08-9
Molecular Formula:C₂₂H₂₂F₃NO₇S
Molecular Weight:501.48
Hs Code.:

Synonyms:7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

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Chemical Property of 7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

There total 4 articles about 7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1351592-05-6
4-(3,4,5-trimethoxybenzyl)-7-ethoxyisoquinolin-8-ol

: 1351592-08-9
7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

Reference yield:

: 492-88-6
3-ethoxysalicylaldehyde

: 1351592-08-9
7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene / 4 h / 150 °C / Inert atmosphere

2.1: ethanol; sodium tetrahydroborate / 1 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride / ethanol / 0.33 h / 100 °C / Microwave irradiation

3.2: pH 7

4.1: triethylamine / N,N-dimethyl-formamide / 0.33 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; ethanol; triethylamine; In ethanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1351592-03-4
(E)-2-((2,2-diethoxyethylimino)methyl)-6-ethoxyrhenol

: 1351592-08-9
7-ethoxy-4-(3,4,5-trimethoxybenzyl)isoquinolin-8-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol; sodium tetrahydroborate / 1 h / 100 °C / Inert atmosphere

2.1: hydrogenchloride / ethanol / 0.33 h / 100 °C / Microwave irradiation

2.2: pH 7

3.1: triethylamine / N,N-dimethyl-formamide / 0.33 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; ethanol; triethylamine; In ethanol; N,N-dimethyl-formamide;