2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione

Base Information

• Chemical Name: 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione
• CAS No.: 496064-23-4
• Molecular Formula: C₃₈H₃₁N₃O₅S
• Molecular Weight: 641.747

Synonyms:2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione

Chemical Property of 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione

Chemical Property:

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Technology Process of 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione

There total 1 articles about 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[3-(4-{[(E)-6-(4-Benzyloxy-phenoxy)-benzothiazol-2-ylimino]-methyl}-phenoxy)-propyl]-isoindole-1,3-dione → 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione (496064-23-4)

Guidance literature:

With sodium tetrahydroborate; In ethanol; toluene; Heating;

DOI:10.1016/j.bmc.2004.05.040

Reference yield: 70.0%

2-(3-(tert-butoxycarbonylamino)propoxy)benzoyl fluoride (496064-27-8) + 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione (496064-23-4) → N-(3-(2-(N-(6-(4-benzyloxyphenoxy)benzothiazol-2-yl)-N-(4-(3-(1,3-dihydro-1,3-dioxoisoindol-2-yl)propoxy)benzyl)carbamoyl)phenoxy)propyl)carbamic acid tert-butyl ester (496064-24-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; at 60 ℃;

DOI:10.1016/j.bmc.2004.05.040

Reference yield: 58.0%

2-methoxybenzoyl fluoride (138421-49-5) + 2-(3-(4-((6-(4-benzyloxyphenoxy)benzothiazol-2-ylamino)methyl)phenoxy)propyl)isoindole-1,3-dione (496064-23-4) → N-(6-(4-benzyloxyphenoxy)benzothiazol-2-yl)-N-(4-(3-(1,3-dihydro-1,3-dioxoisoindol-2-yl)propoxy)benzyl)-2-methoxybenzamide (754992-77-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; at 60 ℃;

DOI:10.1016/j.bmc.2004.05.040

Downstream raw materials:

N-(6-(4-benzyloxyphenoxy)benzothiazol-2-yl)-N-(4-(3-(1,3-dihydro-1,3-dioxoisoindol-2-yl)propoxy)benzyl)-2-methoxybenzamide

N-(3-(2-(N-(6-(4-benzyloxyphenoxy)benzothiazol-2-yl)-N-(4-(3-(1,3-dihydro-1,3-dioxoisoindol-2-yl)propoxy)benzyl)carbamoyl)phenoxy)propyl)carbamic acid tert-butyl ester

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