2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide

Base Information

Chemical Name:2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide
CAS No.:942512-24-5
Molecular Formula:C₂₁H₁₆ClNS
Molecular Weight:349.884
Hs Code.:

Synonyms:2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide

Chemical Property:

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Technology Process of 2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide

There total 2 articles about 2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 942512-16-5
1-bromo-2-[1-(4-chlorophenyl)ethenyl]benzene

: 103-72-0
phenyl isothiocyanate

: 942512-24-5
2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide

Guidance literature:: 1-bromo-2-[1-(4-chlorophenyl)ethenyl]benzene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃;

phenyl isothiocyanate; In diethyl ether; hexane; at 0 ℃;
DOI:10.1246/bcsj.80.763

Reference yield:

: 99585-64-5
(2-bromophenyl)(4-chlorophenyl)methanone

: 942512-24-5
2-[1-(4-chlorophenyl)ethenyl]-N-phenylthiobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 73 percent / tetrahydrofuran / 0 °C

2.1: n-butyllithium / diethyl ether; hexane / 0 °C

2.2: 72 percent / hexane; diethyl ether / 0 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1246/bcsj.80.763