(RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

Base Information

Chemical Name:(RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole
CAS No.:847233-16-3
Molecular Formula:C₃₁H₃₂N₂O₂
Molecular Weight:464.607
Hs Code.:

Synonyms:(RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

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Chemical Property of (RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

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Technology Process of (RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

There total 4 articles about (RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (RS)-4-N-methylamino-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole hydrochloride

: 6078-95-1
4,4-diphenyl-3-butenyl bromide

: 847233-16-3
(RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 120 ℃; for 48h;
DOI:10.1016/j.bmc.2004.10.029

Reference yield:

: 847233-15-2
(RS)-4-[N-(tert-butyloxycarbonyl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

: 847233-16-3
(RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / hydrochloric acid / ethanol / 2 h / 45 °C

2: 85 percent / K₂CO₃; NaI / dimethylformamide / 48 h / 120 °C

With hydrogenchloride; potassium carbonate; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.10.029

Reference yield:

: 100-39-0
benzyl bromide

: 847233-16-3
(RS)-4-[N-(1,1-diphenylbul-1-en-4-yl)-N-methylamino]-3-benzyloxy-4,5,6,7-tetrahydrobenzo[d]isoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / K₂CO₃ / dimethylformamide / 40 °C

2: 90 percent / hydrochloric acid / ethanol / 2 h / 45 °C

3: 85 percent / K₂CO₃; NaI / dimethylformamide / 48 h / 120 °C

With hydrogenchloride; potassium carbonate; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.10.029