C₃₆H₅₂O₆Si₂

Base Information

Chemical Name:C₃₆H₅₂O₆Si₂
CAS No.:1401427-04-0
Molecular Formula:C₃₆H₅₂O₆Si₂
Molecular Weight:636.976
Hs Code.:

C<sub>36</sub>H<sub>52</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₆H₅₂O₆Si₂

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Chemical Property of C₃₆H₅₂O₆Si₂

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Technology Process of C₃₆H₅₂O₆Si₂

There total 10 articles about C₃₆H₅₂O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3839-31-4
dimethyl(phenyl)silyl lithium

: 1401427-03-9
C₂₈H₄₀O₅Si

: 1401427-04-0
C₃₆H₅₂O₆Si₂

Guidance literature:: dimethyl(phenyl)silyl lithium; With diethylzinc; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h; Inert atmosphere;

C₂₈H₄₀O₅Si; In tetrahydrofuran; toluene; at -78 - 0 ℃; for 0.5h; Inert atmosphere;

With MoO₅*pyridine*HMPA; In tetrahydrofuran; toluene; at -78 - -20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ja307207q

Reference yield:

: C₃₁H₅₀O₅Si₂

: 1401427-04-0
C₃₆H₅₂O₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: diethylzinc / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 0 °C / Inert atmosphere

2.3: 0.33 h / -78 - -20 °C / Inert atmosphere

With diethylzinc; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja307207q

Reference yield:

: 40010-11-5,61277-64-3,65942-01-0,81371-52-0,81371-53-1,93714-01-3,108644-64-0,133268-63-0,133268-64-1,143005-10-1,143005-11-2
methyl 3-O-benzyl-α-D-glucopyranoside

: 1401427-04-0
C₃₆H₅₂O₆Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane; toluene / 1.75 h / 45 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 4.5 h / 0 - 20 °C / Inert atmosphere

3.1: dmap / 1,2-dichloro-ethane / 1 h / 50 °C / Inert atmosphere; Sealed tube

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 12 h / 80 °C / Inert atmosphere

5.1: mercury(II) trifluoroacetate / water; acetone / 20 h / 20 °C / Inert atmosphere; Sealed tube

6.1: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

7.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

8.1: titanium tetrachloride / toluene / 1.17 h / -78 °C / Inert atmosphere

8.2: 5 h / -78 - 5 °C / Inert atmosphere

9.1: 1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide / acetonitrile / 3 h / 82 °C / Inert atmosphere

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 20 °C / Inert atmosphere

11.1: diethylzinc / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

11.2: 0.5 h / -78 - 0 °C / Inert atmosphere

11.3: 0.33 h / -78 - -20 °C / Inert atmosphere

With 1H-imidazole; dmap; iodine; diethylzinc; mercury(II) trifluoroacetate; titanium tetrachloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetone; toluene; acetonitrile;
DOI:10.1021/ja307207q