(Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

Base Information

Chemical Name:(Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate
CAS No.:1609548-86-8
Molecular Formula:C₂₁H₁₃F₆NO₄
Molecular Weight:457.329
Hs Code.:

Synonyms:(Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

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Technology Process of (Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

There total 1 articles about (Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 725-89-3
3,5-bistrifluoromethylbenzoic acid

: 1424055-75-3
C₁₂H₁₁NO₃

: 1609548-86-8
(Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.583333h; Autoclave;
DOI:10.1021/ol501051p

Reference yield:

: 1609548-86-8
(Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

: 4-(1-bromo-3-phenylprop-2-yn-1-yl)oxazolidin-2-one

: 4-(1-bromo-3-phenylprop-2-yn-1-yl)oxazolidin-2-one

Guidance literature:: With Fe(NTf₂)2; tetraethylammonium bromide; 2-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)pyridine; In dichloromethane; at 0 ℃; for 2h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1055/s-0034-1378719

Reference yield:

: 1609548-86-8
(Z)-5-phenylpent-2-en-4-yn-1-yl (3,5-bis(trifluoromethyl)benzoyl)oxycarbamate

: anti-4-(1-fluoro-3-phenylprop-2-yn-1-yl)oxazolidin-2-one

: syn-4-(1-fluoro-3-phenylprop-2-yn-1-yl)oxazolidin-2-one

Guidance literature:: With iron(II) tetrafluoroborate hexahydrate; 2-(pyridin-2-yl)-8,8a-dihydro-3aH-indeno[1,2-d]oxazole; triethylamine tris(hydrogen fluoride); ethanaminium,N-(difluoro-λ⁴-sulfanylidene)-N-ethyl-,tetrafluoroborate; In dichloromethane; at 0 - 23 ℃; for 0.166667h; Overall yield = 75 %; diastereoselective reaction; Autoclave; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol501051p