2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

Base Information

Chemical Name:2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline
CAS No.:87880-53-3
Molecular Formula:C₂₀H₂₁N₃O₄S
Molecular Weight:399.47
Hs Code.:

Synonyms:2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

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Chemical Property of 2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

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Technology Process of 2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

There total 7 articles about 2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 22608-86-2
2-acetylamino-4,5-dimethoxybenzaldehyde

: 66299-55-6
3,4-dimethoxy(thiobenzohydrazide)

: 87880-53-3
2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

Guidance literature:: With hydrogenchloride; In ethanol; for 3h; Heating;
DOI:10.1039/P19830002011

Reference yield: 50.0%

: 108-24-7
acetic anhydride

: 87880-55-5
4-acetyl-5-(2-amino-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyl)-Δ²-1,3,4-thiadiazoline

: 87880-56-6
4-acetyl-5-(2-acetylamino-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)-Δ²-1,3,4-thiadiazoline

: 87880-53-3
2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

Guidance literature:: With perchloric acid; In dichloromethane; at 0 ℃;
DOI:10.1039/P19830002011

Reference yield:

: 66299-55-6
3,4-dimethoxy(thiobenzohydrazide)

: 87880-53-3
2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / ethanol / Heating

2: ethanolic HCl / ethanol / Heating

With hydrogenchloride; In ethanol;
DOI:10.1039/P19830002011