(μ3-C(C6H5))Co2MoCp(CO)8

Base Information

Chemical Name:(μ3-C(C6H5))Co2MoCp(CO)8
CAS No.:68185-45-5
Molecular Formula:C₂₀H₁₀Co₂MoO₈
Molecular Weight:592.221
Hs Code.:

Synonyms:(μ3-C(C6H5))Co2MoCp(CO)8

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Chemical Property of (μ3-C(C6H5))Co2MoCp(CO)8

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Technology Process of (μ3-C(C6H5))Co2MoCp(CO)8

There total 9 articles about (μ3-C(C6H5))Co2MoCp(CO)8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₆H₅CC₅H₅(CO)2MoCo(CO)2Co(CO)2As((CH₃)2)Co(CO)2

: 201230-82-2
carbon monoxide

: 68185-45-5
(μ3-C(C6H5))Co2MoCp(CO)8

Guidance literature:: In benzene; byproducts: (AsMe2Co(CO)3)x; CO stream was conducted into the soln. of the cluster compd. for 4.5 h; removing the byproduct by filtration, evapn. in vac.;

Reference yield: 61.0%

: phenylidynetricobalt(I)nonacarbonyl

: Na⁽¹⁺⁾*Mo(C₅H₅)(CO)3^(1-) = NaMo(C₅H₅)(CO)3

: 68185-45-5
(μ3-C(C6H5))Co2MoCp(CO)8

Guidance literature:: In tetrahydrofuran; a soln. of educts in THF was stirred under Ar for 4 h at 20°C;; evapd. in vac. and dried; diethyl ether added twice and dried again to remove residual THF; residue dissolved in hexane; filtered; concd. and crystallized. at -30°C;;

Reference yield: 47.0%

: phenylidynetricobalt(I)nonacarbonyl

: Na⁽¹⁺⁾*Mo(C₅H₅)(CO)3^(1-) = NaMo(C₅H₅)(CO)3

: 68185-45-5
(μ3-C(C6H5))Co2MoCp(CO)8

: μ3-(phenylmethylidyne)-triangulo-(tricarbonylcobalt)bis{dicarbonyl(cyclopentadienyl)molybdenum}(2 Co-Mo, Mo-Mo)

Guidance literature:: In tetrahydrofuran; mixt. of educts are stirred under Ar for 2 d at 60°C;; the residue after evapn. of solvent was extd. with benzene; filtered, concd.; hexane added; chromy. (silica gel/hexan/benzene (3:1), (4:1)); recrystd. from hexane; elem. anal.;;