(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

Base Information

Chemical Name:(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one
CAS No.:85254-20-2
Molecular Formula:C₁₄H₂₅NO₂Si
Molecular Weight:267.443
Hs Code.:

Synonyms:(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

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Technology Process of (3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

There total 1 articles about (3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 53915-69-8
allenyltributylstannane

: 76899-07-5,78963-47-0,78963-48-1,78963-60-7,80951-41-3,81275-02-7,85647-75-2,85954-95-6,92217-74-8,104527-11-9,76855-69-1
(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one

: 85254-20-2
(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(00)80467-0

Reference yield: 97.0%

: 14223-48-4
p-chlorophenyl isoselenocyanate

: 85254-20-2
(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

: 1044259-82-6
C₂₁H₂₉ClN₂O₂SeSi

Guidance literature:: (3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one; With sodium hydride; In tetrahydrofuran; mineral oil; at -10 ℃; for 0.333333h; Inert atmosphere;

p-chlorophenyl isoselenocyanate; In tetrahydrofuran; mineral oil; at -10 ℃; Inert atmosphere;
DOI:10.1021/ol801010y

Reference yield: 96.0%

: 85254-20-2
(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

: 4426-68-0
phenyl isoselenocyanate

: 1044259-83-7
C₂₁H₃₀N₂O₂SeSi

Guidance literature:: (3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one; With sodium hydride; In tetrahydrofuran; mineral oil; at -10 ℃; for 0.333333h; Inert atmosphere;

phenyl isoselenocyanate; In tetrahydrofuran; mineral oil; at -10 ℃; Inert atmosphere;
DOI:10.1021/ol801010y